Compound Identification Method

Official Methods of Moisture Content Determination

Moisture content determination is a crucial aspect of compound identification, influencing various properties and applications. Official methods establish standardized procedures to ensure accuracy and consistency in moisture determination.

Gravitational Method

This method involves drying a sample at a specific temperature and weighing it before and after drying. The weight loss represents the moisture content.

Distillation Method

A sample is subjected to distillation, and the condensed water is collected and measured. The volume of water collected indicates the moisture content.

Karl Fischer Titration

This method uses a chemical titration to determine the moisture content by reacting with a Karl Fischer reagent. The volume of reagent consumed corresponds to the moisture content.

Microwave Drying Method

A sample is heated in a microwave oven to remove moisture. The weight loss is then measured to determine the moisture content.

Other Methods

  • Gas Chromatography
  • Mass Spectrometry
  • Infrared Spectroscopy
  • Nuclear Magnetic Resonance Spectroscopy

Selection of the appropriate method depends on factors such as sample type, accuracy requirements, and available equipment.